|
|
| Index: |
 |
 |
|
Pesticide and Herbicide Analyzes
|
| Category |
Methods
|
Min. Qty.
|
Recommended Containers
|
Required Preservaton
|
Holding Time
|
| -Solid Samples |
| Organochlorine Pesticides & PCB's |
8080
|
30 g
|
Glass Jar w/teflon liner
|
Cool to 4° C
|
14 Days
|
| Organophosphorus Pesticides |
8140
|
30 g
|
Glass Jar w/teflon liner
|
Cool to 4° C
|
14 Days
|
| Herbicides |
8150
|
30 g
|
Glass Jar w/teflon liner
|
Cool to 4° C
|
14 Days
|
| EDB and DBCP |
8260
|
10 g
|
Glass Jar w/teflon liner
|
Cool to 4° C
|
14 Days
|
| Hydrocarbon Analyzes |
| -Aqueous Samples |
|
Hydrocarbon Fingerprint (GC/FID) |
D3328-78
|
1 L
|
2 x L Amber Glass Bottle w/teflon liner
|
Cool to 4° C. Sulphuric acid to pH
<2
|
7 Days
|
| Total Petroleum Hydrocarbons (TPH-IR) |
418.1
|
1 L
|
2 x L Amber Glass Bottle w/teflon liner
|
Cool to 4° C. Sulphuric acid to pH
<2
|
28 Days
|
| Oil and Grease |
413.1, 413.2
|
1 L
|
Cool to 4 deg C. Suphuric acid to pH
<2
|
Cool to 4° C. Sulphuric acid to pH
<2
|
28 Days
|
| Gasoline Range Organics |
8015/API
|
40 mL
|
3 x 40 mL Glass Vials w/teflon sapta
caps
|
Cool to 4° C. HCl to pH <2
|
14 Days
|
| Diesel Range Organics |
8100/API
|
1 L
|
2 x 1 L Amber Glass Bottle w/teflon liner
|
Cool to 4° C. Sulfuric Acid to pH
<2
|
7 Days
|
| -Solid Samples |
| Hydrocarbon Fingerprint (GC/FID) |
D3328-78
|
30 g
|
Glass Jar
|
Cool to 4° C
|
14 Days
|
| Total Petroleum Hydrocarbons (TPH-IR) |
418.1 Modified
|
30 g
|
Glass Jar w/teflon liner
|
Cool to 4° C
|
14 Days
|
| Oil and Grease |
412.1, 413.2
|
30 g
|
Glass Jar w/teflon liner
|
Cool to 4° C
|
14 Days
|
| Gasoline Range Organics |
8015/API
|
10 g
|
1 x 125 mL Glass Vial w/teflon septa cap -or- 2 x 40 mL Glass Vials w/teflon septa caps |
Cool to 4° C
|
14 Days
|
| Diesel Range Organics |
8100/API
|
30 g
|
Glass Jar w/teflon liner
|
Cool to 4° C
|
14 Days
|
|
Metal Analyzes
|
| -Aqueous Samples |
| Total Metals (Except Mercury) |
200s/SM 3111B 6010/7000s
|
100 mL
|
Plastic Bottle
|
Nitric Acid to pH <2. Cool to 4°
C
|
180 Days
|
| Dissolved Metals (Except Mercury) |
200s/SM 3111B. 6010, 7000s
|
100 mL
|
Plastic Bottle
|
Filter First. Nitric Acid to pH <2.
Cool to 4° C
|
180 Days
|
| Total Mercury |
245.1, 7470
|
100 mL
|
Plastic Bottle
|
Nitric Acid to pH <2. Cool to 4°
C
|
28 Days
|
| Dissolved Mercury |
245.1, 7470
|
100 mL
|
Plastic Bottle
|
Filter First. Nitric Acid to pH <2.
Cool to 4° C
|
28 Days
|
| SDWA Lead and Copper Rule |
239.2 SM 3111B
|
1 L
|
1 x 1L Plastic Bottle
|
Cool to 4° C
|
180 Days
|
| Chromium, Hexavalent |
218.1-5
|
200 mL
|
Plastic Bottle
|
Cool to 4° C
|
24 Days
|
| -Solid Samples |
| Total Metals (Except Mercury) |
3010,7000s
|
2 g
|
Class Jar w/teflon liner
|
Cool to 4° C
|
180 Days
|
| Total Mercury |
245.5, 7471
|
0.6 g
|
Class Jar w/teflon liner
|
Cool to 4° C
|
28 Days
|
| Next Page > |