Metals Analyses
| Category |
Methods |
Minimum Qty. |
Recommended Containers |
Required Preservation |
Holding Time |
| Aqueous Samples |
| Total Metals (Except Mercury) |
200s/SM 3111B 6010/7000s |
100 mL |
Plastic Bottle |
Nitric Acid to pH <2. Cool to 4° C |
180 Days |
| Dissolved Metals (Except Mercury) |
200s/SM 3111B. 6010, 7000s |
100 mL |
Plastic Bottle |
Filter First. Nitric Acid to pH <2. Cool to 4° C |
180 Days |
| Total Mercury |
245.1, 7470 |
100 mL |
Plastic Bottle |
Nitric Acid to pH <2. Cool to 4° C |
28 Days |
| Dissolved Mercury |
245.1, 7470 |
100 mL |
Plastic Bottle |
Filter First. Nitric Acid to pH <2. Cool to 4° C |
28 Days |
| SDWA Lead and Copper Rule |
239.2 SM 3111B |
1 L |
1 x 1L Plastic Bottle |
Cool to 4° C |
180 Days |
| Chromium, Hexavalent |
218.1-5 |
200 mL |
Plastic Bottle |
Cool to 4° C |
24 Days |
| Solid Samples |
| Total Metals (Except Mercury) |
3010,7000s |
2 g |
Class Jar w/teflon liner |
Cool to 4° C |
180 Days |
| Total Mercury |
245.5, 7471 |
0.6 g |
Class Jar w/teflon liner |
Cool to 4° C |
28 Days |
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